HuagongsheHuagongshe Chemistry Print Report · For research reference only
Ammonia → N-(2,4,6-tribromophenyl)glycinamide
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Ammonia | HCID 222 | — |
| Reactant | Bromine | HCID 24408 | — |
| Reactant | N-Phenylglycine ethyl ester | HCID 75190 | — |
| Reactant | ethyl N-(2,4,6-tribromophenyl)glycinate | HCID 12659467 | — |
| Solvent | Acetic Acid | HCID 176 | — |
| Solvent | Ethanol | HCID 702 | — |
| Solvent | Water | HCID 962 | — |
| Product | N-(2,4,6-tribromophenyl)glycinamide | HCID 28992175 | — |
Reaction Steps
The ester required for Id, ethyl N-(2,4,6-tribromophenyl)glycinate (IV), was prepared by the reaction of ethyl N-phenylglycinate with bromine in a mixture of water and acetic acid. IV reacted with ammonia in ethanol solution to form N-(2,4,6-tribromophenyl)glycinamide (V).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04352930 |
| Source dataset | uspto-grants-1982_10 |
| ORD ID | ord-12a572969296471cbfd69e364352926a |
| Source note | uspto-grants-1982_10 |