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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 2232847Generated: November 1, 2026

4-Nitrophenol → HCID 14547248, compound

https://huagongshe.com/reaction/2232847

Reaction equation

Participants

RoleNameHCIDCharge
Reactant4-NitrophenolHCID 980—
ReactantDicyclohexylcarbodiimideHCID 10868—
ReactantHCID 14347272HCID 14347272—
SolventCarbon TetrachlorideHCID 5943—
SolventDichloromethaneHCID 6344—
ProductHCID 14547248HCID 1454724882.2%

Reaction Steps

As in Example 115, (2E,4Z)-5-(4-methoxyphenyl)-5-phenyl-2,4-pentadienoic acid (0.85 g) and 4-nitrophenol (0.5 g) in 5 mL of carbon tetrachloride and 5 mL of dichloromethane was treated with 1,3-dicyclohexylcarbodiimide (0.62 g). The mixture was stirred at room temperature for 18 hours and the usual work up furnished 1.0 g of (2E,4Z)-5-(4-methoxyphenyl)-5-phenyl-2,4-pentadienoic acid 4-nitrophenyl ester as an oil.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS04788206
Source datasetuspto-grants-1988_11
ORD IDord-e59261098f4f447da268f0eaf4062680
Source noteuspto-grants-1988_11