HuagongsheHuagongshe Chemistry Print Report · For research reference only
4-Nitrophenol → HCID 14347463, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 4-Nitrophenol | HCID 980 | — |
| Reactant | Dicyclohexylcarbodiimide | HCID 10868 | — |
| Reactant | HCID 14347294 | HCID 14347294 | — |
| Solvent | Dichloromethane | HCID 6344 | — |
| Product | HCID 14347463 | HCID 14347463 | 99.1% |
Reaction Steps
As in Example 115, (2E,4Z)-5-(4-methoxyphenyl)-2,4-decadienoic acid (2.8 g) and 4-nitrophenol (1.71 g) in 20 mL of dichloromethane was reacted with 1,3-dicyclohexylcarbodiimide (2.1 g). The mixture was stirred at room temperature for 18 hours and the usual work up furnished 4.0 g of (2E,4Z)-5-(4-methoxyphenyl)-2,4-decadienoic acid 4-nitrophenyl ester as an oil.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04788206 |
| Source dataset | uspto-grants-1988_11 |
| ORD ID | ord-cf125c4b48d545f2a413fca2ef9dacf1 |
| Source note | uspto-grants-1988_11 |