1-Bromopropane → 1-(4-Methyl-3-nitro-phenyl)-4-propyl-piperazine

HRID 2232903Notes

Reaction equation

HRID 2232903 reaction equation
[CH3:1][C:2]1[CH:7]=[CH:6][C:5]([N:8]2[CH2:13][CH2:12][NH:11][CH2:10][CH2:9]2)=[CH:4][C:3]=1[N+:14]([O-:16])=[O:15].Br[CH2:18][CH2:19][CH3:20]>>[CH3:1][C:2]1[CH:7]=[CH:6][C:5]([N:8]2[CH2:9][CH2:10][N:11]([CH2:18][CH2:19][CH3:20])[CH2:12][CH2:13]2)=[CH:4][C:3]=1[N+:14]([O-:16])=[O:15]

Participants

3

Reactant 2

HCID 78401-BromopropaneHCID 47388041-(4-Methyl-3-nitrophenyl)piperazine

Product 1

HCID 223451841-(4-Methyl-3-nitro-phenyl)-4-propyl-piperazine

Procedure

Beginning with 1-(4-methyl-3-nitro-phenyl)-piperazine and 1-bromopropane, the title compound was recovered by the procedure described in Example 2. MS m/z (rel. intensity, 70 eV) 263 (M+, 26), 234 (bp), 191 (19), 70 (84), 56 (40).

Workup

  1. customthe title compound was recovered by the procedure

Sources & evidence

ORD record
ord-b9e594316d854bc3afad8a39538ed0b4
Source dataset
uspto-grants-2010_05
Patent number
USRE041315E1

Reaction notes

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