1-Bromopropane → HCID 22345170, compound

HRID 2232909Notes

Reaction equation

HRID 2232909 reaction equation
[F:1][C:2]1[CH:7]=[CH:6][C:5]([N:8]2[CH2:13][CH2:12][NH:11][CH2:10][CH2:9]2)=[CH:4][C:3]=1[C:14]([F:17])([F:16])[F:15].Br[CH2:19][CH2:20][CH3:21]>>[F:1][C:2]1[CH:7]=[CH:6][C:5]([N:8]2[CH2:13][CH2:12][N:11]([CH2:19][CH2:20][CH3:21])[CH2:10][CH2:9]2)=[CH:4][C:3]=1[C:14]([F:15])([F:17])[F:16]

Participants

3

Reactant 2

HCID 78401-BromopropaneHCID 22345216HCID 22345216, compound

Product 1

HCID 22345170HCID 22345170, compound

Procedure

Beginning with 1-(4-fluoro-3-trifluoromethyl-phenyl)-piperazine and 1-bromopropane, the title compound was recovered by the procedure described in Example 2. m.p. 238° C. (HCl); MS m/z (rel. intensity, 70 eV) 290 (M+, 17), 261 (70), 190 (34), 70 (bp), 56 (44).

Workup

  1. customthe title compound was recovered by the procedure

Sources & evidence

ORD record
ord-d66416cdec7742b6ade4073c600df31f
Source dataset
uspto-grants-2010_05
Patent number
USRE041315E1

Reaction notes

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