HCID 22345165, compound → HCID 22345206, compound

HRID 2232925Notes

Reaction equation

HRID 2232925 reaction equation
[CH2:1]([N:4]1[CH2:9][CH:8]=[C:7]([C:10]2[CH:15]=[CH:14][C:13]([NH2:16])=[C:12]([C:17]([F:20])([F:19])[F:18])[CH:11]=2)[CH2:6][CH2:5]1)[CH2:2][CH3:3]>CO>[CH2:1]([N:4]1[CH2:9][CH2:8][CH:7]([C:10]2[CH:15]=[CH:14][C:13]([NH2:16])=[C:12]([C:17]([F:20])([F:18])[F:19])[CH:11]=2)[CH2:6][CH2:5]1)[CH2:2][CH3:3]

Participants

3

Reactant 1

HCID 22345165HCID 22345165, compound

Product 1

HCID 22345206HCID 22345206, compound

Reagents, catalysts & solvents 1

HCID 887MethanolSolvent

Procedure

Beginning with 4-(1-Propyl-1,2,3,6-tetrahydropyridine-4-yl)-2-trifluoromethyl-phenylamine, the titled compound was recovered by the procedure described in Preparation 6: MS m/z (rel. intensity, 70 eV)) 286 (M+, 2), 257 (17), 98 (10), 96 (8), 70 (bp), Rf=0.28 (MeOH).

Workup

  1. customthe titled compound was recovered by the procedure
  2. customdescribed in Preparation 6

Sources & evidence

ORD record
ord-5edfabeda1e84341a10f3b54fab6d6df
Source dataset
uspto-grants-2010_05
Patent number
USRE041315E1

Reaction notes

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