HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 131728098, compound → 2-Sulfanylundecanoic acid
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 131728098 | HCID 131728098 | — |
| Solvent | Cadmium selenide | HCID 9837007 | — |
| Product | 2-Sulfanylundecanoic acid | HCID 21932306 | — |
Reaction Steps
In the absence of light, the precipitated CdSe nanocrystals are dissolved in the MUA-methanol solution. The resulting solution is stirred under an Argon flow for about 2 hours to form mercaptoundecanoic acid (MUA)-capped CdSe nanocrystals. Ethyl acetate and ethyl ether are used to precipitate and wash (repeatedly between about 2 and 3 times) the MUA-capped CdSe nanocrystals. Subsequently, the MUA-capped CdSe nanocrystals preferably are dispersed in isopropanol to define a cadmium selenide (CdSe) solution.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07709054B2 |
| Source dataset | uspto-grants-2010_05 |
| ORD ID | ord-fc7e5ccfd3c34d4bb4bd6f75044d3bbd |
| Source note | uspto-grants-2010_05 |