Ethylenediamine → HCID 86594419, compound

HRID 2233011Notes

Reaction equation

HRID 2233011 reaction equation
[CH3:1][N:2]1[C:11]2[C:6](=[CH:7][CH:8]=[CH:9][N:10]=2)[CH:5]=[CH:4][CH:3]1Cl.[CH2:13]([NH2:16])[CH2:14][NH2:15]>>[CH3:1][N:2]1[CH2:3][CH2:4][C:5]2[N:10]=[C:9]([NH:15][CH2:14][CH2:13][NH2:16])[CH:8]=[CH:7][C:6]=2[CH2:11]1

Participants

3

Reactant 2

HCID 3301EthylenediamineHCID 68676574HCID 68676574, compound

Product 1

HCID 86594419HCID 86594419, compound

Conditions

Temperature
138 °C

Procedure

The product from Step A was dissolved in 10 equiv. of ethylenediamine and heated at 138° C. in a sealed tube for 18 h. The excess ethylenediamine was removed by distillation to provide the title compound as a brown oil. MS (M+H)+=207.0.

Workup

  1. customThe excess ethylenediamine was removed by distillation

Sources & evidence

ORD record
ord-b7562078bce94d1f8fd192e8f33737ce
Source dataset
uspto-grants-2010_05
Patent number
US07709473B2

Reaction notes

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