Sodium Carbonate → HCID 58730640, compound

Participants

Reaction Steps

Starting from 1.00 g (1.81 mmol) of the bromide from Example 11A, reaction by general method [D] with 0.33 g (2.18 mmol) of 3-methoxyphenylboronic acid, 0.06 g (0.09 mmol) of bis(triphenylphosphine)palladium(II) chloride and 0.23 g (2.18 mmol) of sodium carbonate in 20 ml of 1,2-dimethoxyethane and 1 ml of water results in 466 mg (44% of theory) of the target compound.

Provenance & Evidence