Hexyl isocyanate → HCID 131728100, compound

HRID 2233529Notes

Reaction equation

HRID 2233529 reaction equation
[C:1]([C:4]1[CH:13]=[CH:12][C:7]2[NH:8][C:9](=[O:11])[O:10][C:6]=2[CH:5]=1)(=[O:3])[CH3:2].N([CH2:17][CH2:18][CH2:19][CH2:20][CH2:21][CH3:22])=C=O>>[C:1]([C:4]1[CH:13]=[CH:12][C:7]2[NH:8][C:9](=[O:11])[O:10][C:6]=2[CH:5]=1)(=[O:3])[CH3:2].[CH3:22][CH2:21][CH:20]([C:9]([NH2:8])=[O:10])[CH2:19][CH2:18][CH3:17]

Participants

3

Reactant 2

HCID 75659Hexyl isocyanateHCID 6890542(3H)-Benzoxazolone, 6-acetyl-

Product 1

HCID 131728100HCID 131728100, compound

Procedure

100 mg (0.565 mmol) of 6-acetyl-3H-benzooxazol-2-one were reacted in analogy to Example 1 with 86.2 mg (0.678 mmol) of 1-isocyanatohexane. Yield: 77 mg (45%), M+H+: 305.15.

Sources & evidence

ORD record
ord-851be38db7ae40bbaa7a789933de04f4
Source dataset
uspto-grants-2010_05
Patent number
US07709513B2

Reaction notes

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