2(3H)-Benzoxazolone → HCID 131728102, compound

HRID 2233531Notes

Reaction equation

HRID 2233531 reaction equation
[O:1]1[C:5]2[CH:6]=[CH:7][CH:8]=[CH:9][C:4]=2[NH:3][C:2]1=[O:10].N([CH2:14][CH2:15][CH2:16][CH2:17][CH2:18][CH3:19])=C=O>O1CCOCC1>[O:10]=[C:2]1[NH:3][C:4]2[CH:9]=[CH:8][CH:7]=[CH:6][C:5]=2[O:1]1.[CH3:19][CH2:18][CH:17]([C:2]([NH2:3])=[O:1])[CH2:16][CH2:15][CH3:14]

Participants

4

Reactant 2

HCID 60432(3H)-BenzoxazoloneHCID 75659Hexyl isocyanate

Product 1

HCID 131728102HCID 131728102, compound

Reagents, catalysts & solvents 1

HCID 312751,4-DioxaneSolvent

Procedure

100 mg (0.74 mmol) of 3H-benzooxazol-2-one were reacted in analogy to Example 1 with 113 mg (0.888 mmol) of 1-isocyanatohexane in dioxane at 80° C. Yield: 163 mg (84%), M+H+: 263.13.

Sources & evidence

ORD record
ord-45252c6b27bd4b2f90dc50f85e20a1c6
Source dataset
uspto-grants-2010_05
Patent number
US07709513B2

Reaction notes

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