HuagongsheHuagongshe Chemistry Print Report · For research reference only
Salicylic acid, hydrazide → Fenadiazole
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Salicylic acid, hydrazide | HCID 13637 | — |
| Reactant | Orthoameisensaureathylester | HCID 5231668 | — |
| Product | Fenadiazole | HCID 13883 | 64.7% |
Reaction Steps
90 g (0.6 mole) of salicylic acid hydrazide and 355.2 g (2.4 moles) of orthoformic acid ethyl ester are refluxed for 22 hours. Excess of the ester is distilled off and the solid residue is recrystallized from ethanol. 62.9 g of colorless crystals (64.7% of theory) are obtained; melting point 112°-113° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04353904 |
| Source dataset | uspto-grants-1982_10 |
| ORD ID | ord-11f395897a36407c812ff3a5df684d20 |
| Source note | uspto-grants-1982_10 |