HuagongsheHuagongshe Chemistry Print Report · For research reference only
Nitric Acid → HCID 18704056, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Nitric Acid | HCID 944 | — |
| Reactant | 5-Methylbenzimidazolone | HCID 223134 | — |
| Product | HCID 18704056 | HCID 18704056 | 99.7% |
Reaction Steps
A mixture of 6-methyl-1,3-dihydro-benzoimidazol-2-one (0.30 g, 2.03 mmol) in 69% nitric acid (5 ml) was stirred over ice for 2 h. The yellow mixture was filtered and washed with water to give (22) as a bright yellow solid (0.39 g, 99.7%).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07709514B2 |
| Source dataset | uspto-grants-2010_05 |
| ORD ID | ord-0fb2da147550416c91416201e814bf90 |
| Source note | uspto-grants-2010_05 |