2-Methylimidazoline → 2-Methyl-1-[2-[(2,6-dimethylphenyl)carbamoyl]ethyl]-2-imidazoline

HRID 223382Notes

Reaction equation

HRID 223382 reaction equation
[CH3:1][C:2]1[CH:7]=[CH:6][CH:5]=[C:4]([CH3:8])[C:3]=1[NH:9][C:10]([CH2:12][CH2:13]Cl)=[O:11].[CH3:15][C:16]1[NH:20][CH2:19][CH2:18][N:17]=1>C(O)C>[CH3:15][C:16]1[N:20]([CH2:13][CH2:12][C:10](=[O:11])[NH:9][C:3]2[C:2]([CH3:1])=[CH:7][CH:6]=[CH:5][C:4]=2[CH3:8])[CH2:19][CH2:18][N:17]=1

Participants

4

Reactant 2

HCID 107982-MethylimidazolineHCID 45508323-Chloro-2',6'-propionoxylidide

Product 1

HCID 204806362-Methyl-1-[2-[(2,6-dimethylphenyl)carbamoyl]ethyl]-2-imidazoline

Reagents, catalysts & solvents 1

HCID 702EthanolSolvent

Procedure

In a manner similar to Ex. IA react 5.29 gm. (0.025 M) of 3-chloro-2',6'-propionoxylidide with 10.53 gm. (0.125 M) of lysidine in 200 ml. of anhydrous ethanol to obtain the title compound.

Workup

  1. customIA react 5.29 gm

Sources & evidence

ORD record
ord-e44169c0ffb44fc6b0d35ca1242c4e68
Source dataset
uspto-grants-1982_10
Patent number
US04353921

Reaction notes

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