HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 86038331, compound → HCID 68580149, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 86038331 | HCID 86038331 | — |
| Solvent | Isopropanol | HCID 3776 | — |
| Product | HCID 68580149 | HCID 68580149 | — |
Reaction Steps
A solution of methyl 6-azidopyridine-2-carboxylate 1-oxide (Intermediate 127, 2.6 g, 13 mmol) in isopropanol was bubbled with nitrogen for 20 minutes followed heating to reflux for 16 hours. The solution was concentrated to a red oil (2.55 g, 99%).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07709503B2 |
| Source dataset | uspto-grants-2010_05 |
| ORD ID | ord-38a91cb9035341019b10e42c5908a4e2 |
| Source note | uspto-grants-2010_05 |