HuagongsheHuagongshe Chemistry Print Report · For research reference only
2-Fluoro-N-(1-methyl-4-piperidinyl)-4-nitrobenzamide → HCID 58009763, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2-Fluoro-N-(1-methyl-4-piperidinyl)-4-nitrobenzamide | HCID 58009769 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | HCID 58009763 | HCID 58009763 | — |
Reaction Steps
2-fluoro-N-(1-methyl-4-piperidyl)-4-nitro-benzamide (Intermediate 62; 1.62 g, 5.8 mmol), 10% Palladium on Carbon (160 mg) and Methanol (50 mL) were combined and stirred at 25 )C under Hydrogen at 5 bar pressure for 16 hours.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07709471B2 |
| Source dataset | uspto-grants-2010_05 |
| ORD ID | ord-e7403525dd70444cbff824b9aef8d436 |
| Source note | uspto-grants-2010_05 |