HuagongsheHuagongshe Chemistry Print Report · For research reference only
Thionyl Chloride → 3-methoxy-4-nitro-benzoyl Chloride
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Thionyl Chloride | HCID 24386 | — |
| Reactant | 3-Methoxy-4-nitrobenzoic acid | HCID 78764 | — |
| Solvent | Toluene | HCID 1140 | — |
| Product | 3-methoxy-4-nitro-benzoyl Chloride | HCID 11127655 | 100% |
Reaction Steps
3-methoxy-4-nitrobenzoic acid (Aldrich; 9 g, 45.65 mmol) was suspended in toluene (90 mL) and thionyl chloride (9.99 mL, 136.95 mmol) added and the mixture heated to reflux for 1 hour. The reaction was evaporated to yield the title compound as a brown solid (9.84 g, 100%).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07709471B2 |
| Source dataset | uspto-grants-2010_05 |
| ORD ID | ord-7221e81745f94a05855b8465ae127515 |
| Source note | uspto-grants-2010_05 |