HuagongsheHuagongshe Chemistry Print Report · For research reference only
1-Pyrrolidineethanamine → 3-methoxy-4-nitro-N-(2-pyrrolidin-1-ylethyl)benzamide
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 1-Pyrrolidineethanamine | HCID 1344 | — |
| Reactant | 3-methoxy-N-[(3R)-1-methylpyrrolidin-3-yl]-4-nitro-benzamide | HCID 68683036 | — |
| Product | 3-methoxy-4-nitro-N-(2-pyrrolidin-1-ylethyl)benzamide | HCID 68686014 | — |
Reaction Steps
The title compound was prepared by an analogous method to the preparation of Intermediate 188, on a 9.28 mmol scale utilising 2-pyrrolidin-1-ylethanamine (Aldrich; 1.06 g, 9.28 mmol), as a brown solid (2.3 g, 85%)
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07709471B2 |
| Source dataset | uspto-grants-2010_05 |
| ORD ID | ord-38db5edb0a63433682c3c0528de4992b |
| Source note | uspto-grants-2010_05 |