HuagongsheHuagongshe Chemistry Print Report · For research reference only
N,N-Dimethyl-1,3-propanediamine → N-(3-dimethylaminopropyl)-3-methoxy-4-nitro-benzamide
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | N,N-Dimethyl-1,3-propanediamine | HCID 7993 | — |
| Reactant | 3-methoxy-N-[(3R)-1-methylpyrrolidin-3-yl]-4-nitro-benzamide | HCID 68683036 | — |
| Product | N-(3-dimethylaminopropyl)-3-methoxy-4-nitro-benzamide | HCID 68681970 | — |
Reaction Steps
The title compound was prepared by an analogous method to the preparation of Intermediate 188, on a 9.28 mmol scale utilising N,N-dimethylpropane-1,3-diamine (Aldrich; 948 mg, 9.28 mmol), as a brown solid (2.33 g, 90%)
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07709471B2 |
| Source dataset | uspto-grants-2010_05 |
| ORD ID | ord-3a4e08784ae34b368270540d56a71ad2 |
| Source note | uspto-grants-2010_05 |