HuagongsheHuagongshe Chemistry Print Report · For research reference only
5-Chloro-2-methoxybenzene-1-sulfonyl chloride → HCID 68697511, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 5-Chloro-2-methoxybenzene-1-sulfonyl chloride | HCID 2734272 | — |
| Reactant | HCID 15984085 | HCID 15984085 | — |
| Product | HCID 68697511 | HCID 68697511 | — |
Reaction Steps
4-{[1-(5-Chloro-2-methoxy-benzenesulfonyl)-2,3-dihydro-1H-indole-6-carbonyl]-amino}-benzoic acid, MS (ISP): m/e=485.2 (M−H), was prepared in analogy to example 30, steps 1 to 6. Step 5 was performed using 5-chloro-2-methoxy-benzenesulfonyl chloride, yielding 4-{[1-(5-chloro-2-methoxy-benzenesulfonyl)-2,3-dihydro-1H-indole-6-carbonyl]-amino}-benzoic acid ethyl ester, which was hydrolyzed in step 6.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07713996B2 |
| Source dataset | uspto-grants-2010_05 |
| ORD ID | ord-0facf3fce6c54982b0e6fd026f9567cd |
| Source note | uspto-grants-2010_05 |