HuagongsheHuagongshe Chemistry Print Report · For research reference only
3-Fluorobenzenesulfonyl Chloride → HCID 68700889, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 3-Fluorobenzenesulfonyl Chloride | HCID 2734258 | — |
| Reactant | HCID 16050420 | HCID 16050420 | — |
| Product | HCID 68700889 | HCID 68700889 | — |
Reaction Steps
4-{[1-(3-Fluoro-benzenesulfonyl)-2,3-dihydro-1H-indole-6-carbonyl]-amino}-benzoic acid, MS (ISP): m/e=439.3 (M−H), was prepared in analogy to example 30, steps 1 to 6. Step 5 was performed using 3-fluoro-benzenesulfonyl chloride, yielding 4-{[1-(3-fluoro-benzenesulfonyl)-2,3-dihydro-1H-indole-6-carbonyl]-amino}-benzoic acid ethyl ester, which was hydrolyzed in step 6.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07713996B2 |
| Source dataset | uspto-grants-2010_05 |
| ORD ID | ord-8426f2a02be7449a9fd84fd919b01fb4 |
| Source note | uspto-grants-2010_05 |