N-bromobutanimide → HCID 59299491, compound

HRID 2235189Notes

Reaction equation

HRID 2235189 reaction equation
[Br:1][C:2]1[CH:7]=[CH:6][C:5]([Cl:8])=[C:4]([CH3:9])[C:3]=1[Cl:10].[Br:11]N1C(=O)CCC1=O>C(OOC(=O)C1C=CC=CC=1)(=O)C1C=CC=CC=1>[Br:1][C:2]1[CH:7]=[CH:6][C:5]([Cl:8])=[C:4]([CH2:9][Br:11])[C:3]=1[Cl:10]

Participants

4

Reactant 2

HCID 67184N-bromobutanimideHCID 148011751-Bromo-2,4-dichloro-3-methylbenzene

Product 1

HCID 59299491HCID 59299491, compoundYield 99.7%

Reagents, catalysts & solvents 1

HCID 7187Benzoyl PeroxideCatalyst

Procedure

By the method in Preparation 5 and using the reagents 1-bromo-2,4-dichloro-3-methyl-benzene (74.4 g, 310 mmol), N-bromosuccinimide (58.0 g, 326 mmol) and benzoyl peroxide (750 mg) affords the title compound as an amber oil (98.5 g, 99%):

Workup

  1. customBy the method in Preparation 5

Sources & evidence

ORD record
ord-4ff5a07d66f74ddfa7c42412c90483b5
Source dataset
uspto-grants-2010_05
Patent number
US07713979B2

Reaction notes

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