2-Oxazolidinone → 3-Pent-4-enoyl-oxazolidin-2-one

HRID 2235196Notes

Reaction equation

[O:1]1[CH2:5][CH2:4][NH:3][C:2]1=[O:6].[C:7](Cl)(=[O:12])[CH2:8][CH2:9][CH:10]=[CH2:11]>>[C:7]([N:3]1[CH2:4][CH2:5][O:1][C:2]1=[O:6])(=[O:12])[CH2:8][CH2:9][CH:10]=[CH2:11]

Participants

Reactant 2

HCID 739492-Oxazolidinone

HCID 42284934-Pentenoyl chloride

Product 1

HCID 107972093-Pent-4-enoyl-oxazolidin-2-oneYield 53%

Procedure

Using the method of preparation 20 and reagents oxazolidin-2-one (10.22 g, 117.3 mmol) and pent-4-enoyl chloride affords 10.62 g (53%) of the title compound as a colorless oil.

Sources & evidence

ORD record: ord-07401c5c2a26493e99799e8383dfc287
Source dataset: uspto-grants-2010_05
DOI: 10.6084/m9.figshare.5104873.v1
Patent number: US07713979B2

Reaction notes

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