Carbon Disulfide → HCID 20263992, compound

HRID 223524Notes

Reaction equation

Cl.[CH:2]([C:4]1[C:9]([OH:10])=[C:8]([CH2:11]O)[C:7]([CH2:13][OH:14])=[CH:6][N:5]=1)=[CH2:3].[OH-].[Na+].C(=S)=[S:18]>>[CH:2]([C:4]1[C:9]([OH:10])=[C:8]([CH2:11][SH:18])[C:7]([CH2:13][OH:14])=[CH:6][N:5]=1)=[CH2:3]

Participants

Reactant 3

HCID 6348Carbon Disulfide

HCID 14798Sodium Hydroxide

HCID 70492662HCID 70492662, compound

Product 1

HCID 20263992HCID 20263992, compound

Procedure

The product from Step F is treated with sodium hydroxide and carbon disulfide as described in Example 1, Step C, to produce 2-vinyl-3-hydroxy-4-mercaptomethyl-5-hydroxymethylpyridine.

Sources & evidence

ORD record: ord-cb841a3385d04e7bb0cc744e2c61b3b3
Source dataset: uspto-grants-1982_10
DOI: 10.6084/m9.figshare.5104873.v1
Patent number: US04355034

Reaction notes

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