HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 223531Generated: October 29, 2026
Water → 2-Methyl-3-hydroxy-4-mercaptomethyl-5-vinylpyridine
https://huagongshe.com/reaction/223531
Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | Water | HCID 962 | — |
| Reactant | Sodium Thiosulfate Pentahydrate | HCID 61475 | — |
| Reactant | 2-Methyl-3-hydroxy-4-chloromethyl-5-vinylpyridine hydrochloride | HCID 20263972 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | 2-Methyl-3-hydroxy-4-mercaptomethyl-5-vinylpyridine | HCID 13066946 | — |
Reaction Steps
A solution of 20 g. of sodium thiosulfate pentahydrate in 15 ml. of water is added to a solution of 18 g. of 2-methyl-3-hydroxy-4-chloromethyl-5-vinylpyridine hydrochloride in 100 ml. of 50% ethanol. The mixture is heated one hour at 75° C., cooled and evaporated to dryness to give Bunte salt of 2-methyl-3-hydroxy-4-mercaptomethyl-5-vinylpyridine, m.p. 198°-200° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
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| Patent number | US04355034 |
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| Source dataset | uspto-grants-1982_10 |
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| ORD ID | ord-03aea08d8999493d94f452f08d695aa3 |
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| Source note | uspto-grants-1982_10 |
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