HCID 20263934, compound → HCID 20263985, compound

HRID 223533Notes

Reaction equation

HRID 223533 reaction equation
[CH3:1][C:2]1[CH:7]=[C:6]([CH2:8][O:9][C:10](=[O:12])[CH3:11])[C:5]([CH2:13][OH:14])=[CH:4][N:3]=1>N1C=CC=CC=1.[O-2].[O-2].[O-2].[Cr+6]>[CH3:1][C:2]1[CH:7]=[C:6]([CH2:8][O:9][C:10](=[O:12])[CH3:11])[C:5]([CH:13]=[O:14])=[CH:4][N:3]=1

Participants

4

Reactant 1

HCID 20263934HCID 20263934, compound

Product 1

HCID 20263985HCID 20263985, compound

Reagents, catalysts & solvents 2

HCID 10219390chromium (VI) trioxideCatalystHCID 1049PyridineSolvent

Procedure

This product is prepared by oxidation of 2-methyl-B 4-acetoxymethyl-5-hydroxymethylpyridine (from Step A) with chromium trioxide in pyridine by the procedure substantially as described in Example 11, Step A.

Sources & evidence

ORD record
ord-a45a77e39c04402f942d8b54b4d3ce8a
Source dataset
uspto-grants-1982_10
Patent number
US04355034

Reaction notes

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