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HRID2235399

反应详情

EQUATION

反应方程式

HRID 2235399 的结构方程式

REACTANTS

反应物

2
结构：CCCCN1C(=O)C(C)(C)c2cc(N)c([N+](=O)[O-])cc21
HCID17802733

未命名化合物

结构：CC(C)Oc1ccc(CCC(=O)Cl)cc1
HCID23092688

未命名化合物

PRODUCTS

生成物

1
结构：CCCCN1C(=O)C(C)(C)c2cc(NC(=O)CCc3ccc(OC(C)C)cc3)c([N+](=O)[O-])cc21
HCID23092663

未命名化合物

PROCEDURE

实验过程

N-(1-Butyl-3,3-dimethyl-6-nitro-2-oxo-2,3-dihydro-1H-indol-5-yl)-3-(4-isopropoxy-phenyl)-propionamide is prepared from A4 (500 mg) and 3-(4-isopropoxy-phenyl)-propionyl chloride (1.01 g; 5.5 mmol) as described in Example 1a. The crude material is purified by flash chromatography eluting with light petroleum/EtOAc (6:1) to give the compound (791 mg).

WORKUP

后处理

  1. customThe crude material is purified by flash chromatography
  2. washeluting with light petroleum/EtOAc (6:1)