Allyl Alcohol → HCID 59300967, compound

HRID 2235428Notes

Reaction equation

HRID 2235428 reaction equation
[CH3:1][O:2][C:3](=[O:25])[NH:4][C:5]1[NH:24][C:8]2=[CH:9][C:10]3[C:11]([CH3:23])([CH3:22])[C:12](=[O:21])[N:13]([CH2:16][CH2:17][CH2:18][CH2:19][CH3:20])[C:14]=3[CH:15]=[C:7]2[N:6]=1.[CH2:26](O)[CH:27]=C>>[CH2:1]([O:2][C:3](=[O:25])[NH:4][C:5]1[NH:24][C:8]2=[CH:9][C:10]3[C:11]([CH3:23])([CH3:22])[C:12](=[O:21])[N:13]([CH2:16][CH2:17][CH2:18][CH2:19][CH3:20])[C:14]=3[CH:15]=[C:7]2[N:6]=1)[CH:26]=[CH2:27]

Participants

3

Reactant 2

HCID 7858Allyl AlcoholHCID 59300957HCID 59300957, compound

Product 1

HCID 59300967HCID 59300967, compound

Conditions

Temperature
120 °C

Procedure

A suspension of (7,7-dimethyl-6-oxo-5-pentyl-1,5,6,7-tetrahydro-imidazo[4,5-f]indol-2-yl)-carbamic acid methyl ester (150 mg) in allyl alcohol (2 ml) is heated in a microwave apparatus at 120° C. for 20 min. The mixture is evaporated to give the desired compound (161 mg).

Workup

  1. customThe mixture is evaporated

Sources & evidence

ORD record
ord-6f83e7f2b2b749f3876da99643106b5e
Source dataset
uspto-grants-2010_05
Patent number
US07714010B2

Reaction notes

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