HCID 15563288, compound → HCID 178477440, compound

Participants

Reaction Steps

A solution of B30 (0.73 g) and N-(bis-methylsulfanyl-methylene)-benzamide (0.72 g; 2.70 mmol) in dry N,N-dimethylformamide (35 ml) is stirred at 80° C. for 18 h. The mixture is evaporated to dryness and the residue is purified by preparative RP-MPLC eluted with MeCN/water to yield the desired compound (0.76 g).

Provenance & Evidence