HCID 15563288, compound → HCID 178429332, compound

Participants

Reaction Steps

A solution of B37 (190 mg) and N-(bis-methylsulfanyl-methylene)-benzamide (150 mg; 0.67 mmol) in dry N,N-dimethylformamide (3 ml) is stirred at 150° C. for 24 h. The mixture is evaporated to dryness and the residue is purified by preparative RP-HPLC eluted with MeCN/water to yield the desired compound (84.2 mg).

Provenance & Evidence