Propanal → HCID 58896519, compound

Participants

Reaction Conditions

Reaction Steps

To 0.125 g (0.44 mmol) of N2-mesityl-1,3-benzothiazole-2,7-diamine and 0.16 mL (2.2 mmol) of propionaldehyde in 5 mL of dichloroethane was added one drop of glacial acetic acid and 0.28 g (1.3 mmol) of sodium triacetoxyborohydride. The mixture was heated to 50° C. for 1 h and concentrated in vacuo. The crude solid was purified by flash chromatography eluting with a 2% methanol/dichloromethane mixture to give 0.016 g (10%) of the title compound as a tan powder.

Provenance & Evidence