反应详情

A mixture of 2-(mesitylamino)-5-nitro-N,N-dipropyl-1,3-benzothiazole-7-carboxamide (61 mg, 0.139 mmol) and 10% Pd on carbon (30 mg) in ethanol (10 ml) was hydrogenated for 4 h. The catalyst was removed by filtration through Celite. The filtrate was concentrated under vacuum. The residue was purified by chromatography eluting with 20% AcOEt in n-hexane to afford 40 mg of the title compound.

1. customThe catalyst was removed by filtration through Celite
2. concentrationThe filtrate was concentrated under vacuum
3. customThe residue was purified by chromatography
4. washeluting with 20% AcOEt in n-hexane