HuagongsheHuagongshe Chemistry Print Report · For research reference only
Methyldichlorosilane → Silane, dichlorodecylmethyl-
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Methyldichlorosilane | HCID 6376 | — |
| Reactant | 1-Decene | HCID 13381 | — |
| Catalyst | Chloroplatinic acid | HCID 61859 | — |
| Solvent | Isopropanol | HCID 3776 | — |
| Product | Silane, dichlorodecylmethyl- | HCID 87434 | 94% |
Reaction Steps
2.25 Parts of methyl dichlorosilane, 4.04 parts of 1-decene and a solution containing about 0.0005 part of chloroplatinic acid catalyst in 0.006 part of 2-propanol were charged to a reaction vessel and heated to about 100°-120° C. for six hours. The product was vacuum distilled at 110°-114° C. at 1-3 Torr. 4.7 Parts (94% yield) of methyl decyl dichlorosilane was obtained.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04355062 |
| Source dataset | uspto-grants-1982_10 |
| ORD ID | ord-111dd210d57e425787cb6ff3d4b6e9fa |
| Source note | uspto-grants-1982_10 |