HRID2235587

反应详情

EQUATION

反应方程式

REACTANTS

反应物

结构：O=C(C[C@@H](c1ccc(OCc2ccccc2)cc1)C1C=CON1)N1C(=O)OC[C@@H]1Cc1ccccc1

HCID67330499

未命名化合物

PRODUCTS

生成物

结构：O=C(C[C@@H](c1ccc(O)cc1)C1C=CON1)N1C(=O)OC[C@@H]1Cc1ccccc1

HCID67329489

未命名化合物

收率 90.3%

AUXILIARIES

试剂、催化剂与溶剂

催化剂HCID23938

Palladium

溶剂HCID702

Ethanol

C2H6O

PROCEDURE

实验过程

Compound 9.1 (136 mg) and a catalytic amount of Pd/C in EtOH (2 mL) was stirred at room temperature under 1 atm of H2 for 2.5 hours. The catalyst was removed by filtration, and the filtrate was concentrated to give 9.2 (100 mg). MS ESI (pos.) m/e: 395 (M+H).

WORKUP

后处理

customThe catalyst was removed by filtration
concentrationthe filtrate was concentrated