HCID 24898113, compound → HCID 24898772, compound

Participants

Reaction Steps

Compound 37 was synthesized from compound 35 using the procedure described above for the preparation of 23. 1H NMR (CD3CN) δ 1.25 (d, J=6.9 Hz, 6H), 2.96 (dd, J=7.4, 16.4 Hz, 1H), 3.20 (dd, J=7.4, 16.4 Hz, 1H), 3.34 (m, 1H), 4.56 (m, 1H), 5.09 (s, 2H), 6.27 (d, J=1.7 Hz, 1H), 6.97 (d, J=6.6 Hz, 2H), 7.25 (d, J=6.6 Hz, 2H), 7.37 (s, 1H), 7.42 (d, J=8.1 Hz, 1H), 7.48 (d, J=8.1 Hz, 1H), 8.45 (d, J=1.7 Hz, 1H). MS ESI (pos.) m/e: 450 (M+H).

Provenance & Evidence