HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydrochloric Acid → HCID 67067275, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydrochloric Acid | HCID 313 | — |
| Reactant | HCID 67067393 | HCID 67067393 | — |
| Solvent | Acetic Acid | HCID 176 | — |
| Solvent | Ethyl Acetate | HCID 8857 | — |
| Product | HCID 67067275 | HCID 67067275 | 199.8% |
Reaction Steps
A solution of 4 N hydrochloric acid in acetic acid (3 mL) was added to a solution of tert-butyl N′-[5-chloro-2-(2,4,6-trifluorophenyl)pentanoyl]hydrazinecarboxylate (333 mg) in ethyl acetate (3 mL), and the reaction solution was stirred at room temperature for 15 hours. The reaction solution was concentrated under reduced pressure to obtain 277 mg of the title compound. The property value of the compound is as follows.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07713993B2 |
| Source dataset | uspto-grants-2010_05 |
| ORD ID | ord-60e8cb9e73194688871e8dddc8deda36 |
| Source note | uspto-grants-2010_05 |