HuagongsheHuagongshe Chemistry Print Report · For research reference only
(3-Nitrophenoxy)acetic acid → (3-Aminophenoxy)acetic acid
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | (3-Nitrophenoxy)acetic acid | HCID 74656 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Solvent | HCID 87166746 | HCID 87166746 | — |
| Product | (3-Aminophenoxy)acetic acid | HCID 235515 | — |
Reaction Steps
(3-Nitro-phenoxy)-acetic acid (1.978 g; 10.0 mmol) was reduced by catalytic hydrogenation (10% Pd—C; 45 psi H2) in AcOH-EtOH-MeOH then filtered through diatomaceous earth and concd yielding the title aniline. LC-MS 168 ([M+H]+).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07714022B2 |
| Source dataset | uspto-grants-2010_05 |
| ORD ID | ord-b630d5844d374c4ab61135f63f63cecf |
| Source note | uspto-grants-2010_05 |