HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 131727223, compound → HCID 131727224, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 131727223 | HCID 131727223 | — |
| Catalyst | HCID 178418390 | HCID 178418390 | — |
| Solvent | Ethanol | HCID 702 | — |
| Solvent | HCID 178418361 | HCID 178418361 | — |
| Product | HCID 131727224 | HCID 131727224 | — |
Reaction Steps
72.8 mg of palladium carbon (10% w/v) was added to 72.8 mg (0.171 mmol) of (1R)-N-{2-[4-(5H-dibenzo[a,d] [7]annulen-5-ylidene)-1-piperidinyl]-2-oxoethyl}-2,2-dimethylcyclopropanecarboxyamide in 10 ml of ethanol, and they were stirred at 4.0 MPa in hydrogen gas atmosphere overnight. After the filtration, the solvent was evaporated under reduced pressure to obtain the title compound.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07713957B2 |
| Source dataset | uspto-grants-2010_05 |
| ORD ID | ord-42224e195226490ea3517f9f0141594f |
| Source note | uspto-grants-2010_05 |