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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 2235989Generated: October 30, 2026

HCID 131727223, compound → HCID 131727224, compound

https://huagongshe.com/reaction/2235989

Reaction equation

Participants

RoleNameHCIDCharge
ReactantHCID 131727223HCID 131727223—
CatalystHCID 178418390HCID 178418390—
SolventEthanolHCID 702—
SolventHCID 178418361HCID 178418361—
ProductHCID 131727224HCID 131727224—

Reaction Steps

72.8 mg of palladium carbon (10% w/v) was added to 72.8 mg (0.171 mmol) of (1R)-N-{2-[4-(5H-dibenzo[a,d] [7]annulen-5-ylidene)-1-piperidinyl]-2-oxoethyl}-2,2-dimethylcyclopropanecarboxyamide in 10 ml of ethanol, and they were stirred at 4.0 MPa in hydrogen gas atmosphere overnight. After the filtration, the solvent was evaporated under reduced pressure to obtain the title compound.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS07713957B2
Source datasetuspto-grants-2010_05
ORD IDord-42224e195226490ea3517f9f0141594f
Source noteuspto-grants-2010_05