Butyryl chloride → HCID 11567156, compound

HRID 2236083Notes

Reaction equation

[C:1]([C:3]1[C:11]2[CH2:10][CH2:9][NH:8][CH2:7][C:6]=2[S:5][C:4]=1[NH:12][C:13](=[O:22])[C:14]1[CH:19]=[CH:18][CH:17]=[C:16]([O:20][CH3:21])[CH:15]=1)#[N:2].[C:23](Cl)(=[O:27])[CH2:24][CH2:25][CH3:26]>>[C:23]([N:8]1[CH2:9][CH2:10][C:11]2[C:3]([C:1]#[N:2])=[C:4]([NH:12][C:13](=[O:22])[C:14]3[CH:19]=[CH:18][CH:17]=[C:16]([O:20][CH3:21])[CH:15]=3)[S:5][C:6]=2[CH2:7]1)(=[O:27])[CH2:24][CH2:25][CH3:26]

Participants

Reactant 2

HCID 8855Butyryl chloride

HCID 59301482HCID 59301482, compound2×

Product 1

HCID 11567156HCID 11567156, compound

Procedure

Prepared according to general procedure A starting from N-(3-cyano-4,5,6,7-tetrahydro-thieno[2,3-c]pyridin-2-yl)-3-methoxybenzamide (compound B3) and butyryl chloride.

Workup

customPrepared

Sources & evidence

ORD record: ord-c0709c5fc7c9433cb633dee131e54744
Source dataset: uspto-grants-2010_05
DOI: 10.6084/m9.figshare.5104873.v1
Patent number: US07714134B2

Reaction notes

Loading…