L-Valine → HCID 23683721, compound

HRID 2236131Notes

Reaction equation

HRID 2236131 reaction equation
[NH2:1][C@H:2]([C:6]([OH:8])=[O:7])[CH:3]([CH3:5])[CH3:4].[OH-].[Na+:10]>O>[NH2:1][CH:2]([CH:3]([CH3:5])[CH3:4])[C:6]([O-:8])=[O:7].[Na+:10]

Participants

4

Reactant 2

HCID 6287L-ValineHCID 14798Sodium Hydroxide

Product 1

HCID 23683721HCID 23683721, compound

Reagents, catalysts & solvents 1

HCID 962WaterSolvent

Procedure

Separately, in a single-necked, round bottomed flask, equipped with a magnetic stirrer, 5.86 g (50 mmol) of Valine is dissolved in 200 ml of water. To this is added 55 ml of 1M sodium hydroxide with vigorous stirring, until heat production ceases. At this point the water is removed by evaporation to yield the carboxylate salt, sodium 2-amino-3-methylbutanoate, shown below.

Workup

  1. customSeparately, in a single-necked, round bottomed flask, equipped with a magnetic stirrer
  2. temperatureuntil heat production ceases
  3. customAt this point the water is removed by evaporation

Sources & evidence

ORD record
ord-a150d8152298409ba7705617fb573e52
Source dataset
uspto-grants-2010_05
Patent number
US07714154B2

Reaction notes

Loading…