HuagongsheHuagongshe Chemistry Print Report · For research reference only
1-methyl-3-phenyl-1H-pyrazole-5-carboxylic acid → HCID 59301315, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 1-methyl-3-phenyl-1H-pyrazole-5-carboxylic acid | HCID 7537625 | — |
| Reactant | N2-(2-methoxyethyl)-N2-methylpyridine-2,5-diamine | HCID 52937159 | — |
| Product | HCID 59301315 | HCID 59301315 | — |
Reaction Steps
With a procedure similar to example 16 above, 2-methyl-5-phenyl-2H-pyrazole-3-carboxylic acid {6-[(2-methoxy-ethyl)-methyl-amino]-pyridin-3-yl}-amide was prepared from 2-methyl-5-phenyl-2H-pyrazole-3-carboxylic acid (made by hydrolysis of the corresponding commercially available ethyl ester) and N2-(2-methoxy-ethyl)-N2-methyl-pyridine-2,5-diamine. LCMS calcd for C20H23N5O2 (m/e) 365, obsd 366 (M+H). The NMR spectrum obtained on the sample is compatible with its structure.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07714126B2 |
| Source dataset | uspto-grants-2010_05 |
| ORD ID | ord-c105ba16f6274f5ea2bea2a336c668c0 |
| Source note | uspto-grants-2010_05 |