HuagongsheHuagongshe Chemistry Print Report · For research reference only
5-methyl-2-phenyl-2H-1,2,3-triazole-4-carboxylic acid → 5-methyl-2-phenyl-2H-[1,2,3]triazole-4-carboxylic acid {6-[(2-methoxy-ethyl)-methyl-amino]-pyridin-3-yl}-amide
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 5-methyl-2-phenyl-2H-1,2,3-triazole-4-carboxylic acid | HCID 519936 | — |
| Reactant | N2-(2-methoxyethyl)-N2-methylpyridine-2,5-diamine | HCID 52937159 | — |
| Product | 5-methyl-2-phenyl-2H-[1,2,3]triazole-4-carboxylic acid {6-[(2-methoxy-ethyl)-methyl-amino]-pyridin-3-yl}-amide | HCID 59301296 | — |
Reaction Steps
With a procedure similar to example 16 above, 5-methyl-2-phenyl-2H-[1,2,3]triazole-4-carboxylic acid {6-[(2-methoxy-ethyl)-methyl-amino]-pyridin-3-yl}-amide was prepared from 5-methyl-2-phenyl-2H-[1,2,3]triazole-4-carboxylic acid and N2-(2-methoxy-ethyl)-N2-methyl-pyridine-2,5-diamine. LCMS calcd for C19H22N6O2 (m/e) 366, obsd 367 (M+H). The NMR spectrum obtained on the sample is compatible with its structure.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07714126B2 |
| Source dataset | uspto-grants-2010_05 |
| ORD ID | ord-1c0caff673164f239654c419e96b2537 |
| Source note | uspto-grants-2010_05 |