HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydrochloric Acid → HCID 73665701, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydrochloric Acid | HCID 313 | — |
| Reactant | Hydroxylamine, sulfate (1:1) | HCID 159255 | — |
| Reactant | HCID 54325297 | HCID 54325297 | — |
| Solvent | Water | HCID 962 | — |
| Product | HCID 73665701 | HCID 73665701 | 134.8% |
Reaction Steps
The procedure described in Example 1(b) is repeated, except that 110 g (0.5 mol) of 3,3,12,12-tetramethyl-1-aza-1,5,9-cyclododecatriene, 41 g (0.25 mol) of hydroxylamine sulfate, 50 ml of concentrated hydrochloric acid and 250 ml of water are used. Distillation yields 85 g (0.337 mol) of 2,2,11,11-tetramethyl-11-amino-undeca-4,8-dienal oxime; yield 67.4% of theory; boiling point 130° C./7 Pa.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04355177 |
| Source dataset | uspto-grants-1982_10 |
| ORD ID | ord-33af1bdbefb641c29d8fcdb208c684dd |
| Source note | uspto-grants-1982_10 |