HuagongsheHuagongshe Chemistry Print Report · For research reference only
1-Butyl-4-chloromethyl-2-methoxy-benzene → 4-Azidomethyl-1-butyl-2-methoxy-benzene
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 1-Butyl-4-chloromethyl-2-methoxy-benzene | HCID 59300216 | — |
| Reactant | 4-Azidomethyl-2-methoxy-biphenyl | HCID 59300273 | — |
| Product | 4-Azidomethyl-1-butyl-2-methoxy-benzene | HCID 59300153 | 36% |
Reaction Steps
Following the same procedure for the preparation of 4-Azidomethyl-2-methoxy-biphenyl, the title compound is prepared from 1-Butyl-4-chloromethyl-2-methoxy-benzene (crude material from the previous step) in 36% yield (overall yield for 4 steps).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07713994B2 |
| Source dataset | uspto-grants-2010_05 |
| ORD ID | ord-305d1ae7fdbf442182c910cbf7f01e89 |
| Source note | uspto-grants-2010_05 |