HuagongsheHuagongshe Chemistry Print Report · For research reference only
Dimethylformamide → HCID 178463977, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Dimethylformamide | HCID 6228 | — |
| Reactant | N,N-Diethyl-1,4-butanediamine | HCID 117976 | — |
| Reactant | 4-methoxymethylene-6-bromo-4H-isoquinoline-1,3-dione | HCID 68692764 | — |
| Solvent | Diethyl Ether | HCID 3283 | — |
| Product | HCID 178463977 | HCID 178463977 | 26% |
Reaction Steps
A mixture of 6-bromo-4-(methoxymethylene)-isoquinoline-1,3(2H,4H)-dione (70.5 mg, 0.25 mmole), dimethylformamide (2 mL) and N1,N1-diethylbutane-1,4-diamine (36.1 mg, 0.25 mmole) is stirred at room temperature for one hour. The reaction mixture is diluted with ether, filtered and washed with fresh ether and dried to give a light brown solid, 26.0 mg, (26% yield) MS (ES+): 394.2, (M+H).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07713994B2 |
| Source dataset | uspto-grants-2010_05 |
| ORD ID | ord-d37d5508efe64bbe8f3571d79a0e39a3 |
| Source note | uspto-grants-2010_05 |