Ammonia → HCID 54522366, compound

HRID 223729Notes

Reaction equation

HRID 223729 reaction equation
C([S:4][CH2:5][C:6]([N:8]1[CH2:15][C:14]([OH:23])([CH2:16][C:17]2[CH:22]=[CH:21][CH:20]=[CH:19][CH:18]=2)[CH2:13][C@H:9]1[C:10]([OH:12])=[O:11])=[O:7])(=O)C.N>>[OH:23][C:14]1([CH2:16][C:17]2[CH:22]=[CH:21][CH:20]=[CH:19][CH:18]=2)[CH2:15][N:8]([C:6](=[O:7])[CH2:5][SH:4])[C@H:9]([C:10]([OH:12])=[O:11])[CH2:13]1

Participants

3

Reactant 2

HCID 222AmmoniaHCID 53883906HCID 53883906, compound

Product 1

HCID 54522366HCID 54522366, compound

Procedure

The product from part (b) is treated with concentrated ammonia according to the procedure of Example 2 to yield 4-hydroxy-1-(2-mercapto-1-oxoethyl)-4-(phenylmethyl)-L-proline.

Sources & evidence

ORD record
ord-7096b6271e82411aa1a02f4415733087
Source dataset
uspto-grants-1982_10
Patent number
US04356182

Reaction notes

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