Potassium bis(trimethylsilyl)amide → HCID 59302569, compound

Participants

Reaction Steps

MePPh3 Br (785 mg, 2.2 mmol) was dissolved in 7 mL THF and treated with KHMDS (408 mg, 2.04 mmol). After stirring for 30 minutes, the product of step d) (350 mg, 1.5 mmol) was added as a solution in 3 mL THF. After stirring for 1 hour, the reaction was diluted with EtOAc and washed with water. The organic layer was concentrated and the product was purified by silica gel chromatography (EtOAc/Hex-gradient) to give 188 mg of the subtitle compound.

Provenance & Evidence