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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 223755Generated: October 25, 2026

Ethyl p-methylbenzenesulfonate → 3-Ethyl-2-(ethylsulfanyl)-1,3-benzothiazol-3-ium 4-methylbenzene-1-sulfonate

https://huagongshe.com/reaction/223755

Reaction equation

Participants

RoleNameHCIDCharge
ReactantEthyl p-methylbenzenesulfonateHCID 6638—
ReactantHCID 178418395HCID 178418395—
SolventEthanolHCID 702—
Product3-Ethyl-2-(ethylsulfanyl)-1,3-benzothiazol-3-ium 4-methylbenzene-1-sulfonateHCID 14090547—

Reaction Conditions

Temperature150 °C

Reaction Steps

A mixture of 3.3 g of 2-mercaptobenzothiazole and 10.0 g of ethyl p-toluenesulfonate was heated to 150° C. to react them for 6 hours. The reaction product was cooled to 80° C. and then 30 ml of ethanol was added to it, thereby producing an ethanol solution of 2-ethylmercapto-3-ethylbenzothiazolium p-toluenesulfonate.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS04356247
Source datasetuspto-grants-1982_10
ORD IDord-fab06d8802f34d2882e5fc578177755c
Source noteuspto-grants-1982_10