HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 59700729, compound → 4-(Pentyloxy)-3-(trifluoromethyl)aniline
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 59700729 | HCID 59700729 | — |
| Reactant | HCID 178418361 | HCID 178418361 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | 4-(Pentyloxy)-3-(trifluoromethyl)aniline | HCID 17605571 | 101.1% |
Reaction Steps
A solution of 4-Nitro-1-pentyloxy-2-trifluoromethyl-benzene (1.2 g, 4.8 mmole) and 0.1 g of 10% Palladium on activated carbon in 40 mL of ethanol is hydrogenated with hydrogen balloon at room temperature overnight. Filtration and concentration gave a pink oil 1.2 g (100%) of 4-Pentyloxy-3-trifluoromethyl-phenylamine MS: 248 (M+1).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07718671B2 |
| Source dataset | uspto-grants-2010_05 |
| ORD ID | ord-cc64676e475140a8b5e4502d6b57e198 |
| Source note | uspto-grants-2010_05 |