HuagongsheHuagongshe Chemistry Print Report · For research reference only
1-Naphthalenesulfonyl chloride → HCID 10229358, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 1-Naphthalenesulfonyl chloride | HCID 66560 | — |
| Reactant | HCID 22272520 | HCID 22272520 | — |
| Product | HCID 10229358 | HCID 10229358 | — |
Reaction Steps
The compound was synthesized from N-{2-amino-5-(4-t-butyloxycarbonyl-1,4-diazepan-1-yl)-phenyl}methanesulfonamide and 1-napthalenesulfonylchloride (103 mg, 0.455 mmol) to give before Boc-deprotection 150 mg of a purple solid. M+ 1 475.1 Calcd 474.14.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07718650B2 |
| Source dataset | uspto-grants-2010_05 |
| ORD ID | ord-bb388df2fb80485d84e1a3b1120f0e71 |
| Source note | uspto-grants-2010_05 |